Jeffrey, as per my evaporation email, I've had problems with resistive=
evaportation of Ti onto SU-8 due to sample heating. I don't think the=
light from my filaments exposes the Ti, as the dep rate from the Ti=
quickly covers the SU-8 and blocks any further photoabsorption. But if you=
accidentally hard bake the SU-8 during the dep, it won't develop out the=
unexposed regions. Monitor your sample with a thermocouple or a thermister=
if possible.=20
I've been using a little dimpled tungsten boat heater or canoes for Ti.=
Works fine as long as you heat them fast, dep fast and stop fast.=
Resistive evaporation makes a lot of heat from that big ohmically heated=
filament. Ebeam at least mostly just heats the slug of Ti.=20
As for undeveloped SU-8, I've noticed that metal over unexposed SU-8 tends=
to be a little 'waffley' or 'crinkley' compared to the metal over the=
exposed SU-8.=20
Oh, and you *must* do a post-exposure bake... or the undensified SU-8 may=
bubble on pump down. (I forgot once!)=20
-- Jon
---- Message from "Yue Mun Pun, Jeffrey" at=
2007-03-03 15:52:56 ------
>Brent,
>Thanks for the recommendation. Yes, I did try Chromium, which is not as=
easy compared to Titanium either. And I know that Chromium is a good=
adhesion layer for gold too. The reason for using to Titanium is because=
Chromium inhibits Poymerase Chain Reaction, while Titanium is=
biocompatible. However, I need to evaporate Titanium on uncrosslinked=
SU-8, which is why I am trying to thermally evaporate Titanium on SU-8. I=
am well aware that Titanium is tough to thermally evaporate. However, if=
uncrosslinked SU-8 2050 is safe from being crosslinked when Titanium is=
being deposited in an e-beam evaporator, I would gladly evaporate Titanium=
in the e-beam evaporator, which is easier by far.